<?xml version="1.0" encoding="ISO-8859-1"?><article xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance">
<front>
<journal-meta>
<journal-id>0120-2804</journal-id>
<journal-title><![CDATA[Revista Colombiana de Química]]></journal-title>
<abbrev-journal-title><![CDATA[Rev.Colomb.Quim.]]></abbrev-journal-title>
<issn>0120-2804</issn>
<publisher>
<publisher-name><![CDATA[Departamento de Química,  Universidad Nacional de Colombia.]]></publisher-name>
</publisher>
</journal-meta>
<article-meta>
<article-id>S0120-28042017000100060</article-id>
<title-group>
<article-title xml:lang="es"><![CDATA[Síntesis de monetita pura por reacción heterogénea ácido-base]]></article-title>
<article-title xml:lang="en"><![CDATA[Synthesis of pure monetite by heterogeneous acid-base reaction]]></article-title>
<article-title xml:lang="pt"><![CDATA[Síntese de monetita pura por reação heterogênea ácido-base]]></article-title>
</title-group>
<contrib-group>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Cárdenas]]></surname>
<given-names><![CDATA[Davier Olarte]]></given-names>
</name>
<xref ref-type="aff" rid="Aff"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Moreno Aldana]]></surname>
<given-names><![CDATA[Luis Carlos]]></given-names>
</name>
<xref ref-type="aff" rid="Aff"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Delgado Mejía]]></surname>
<given-names><![CDATA[Edgar]]></given-names>
</name>
<xref ref-type="aff" rid="Aff"/>
</contrib>
</contrib-group>
<aff id="Af1">
<institution><![CDATA[,Universidad Nacional de Colombia Departamento de Química ]]></institution>
<addr-line><![CDATA[Bogotá ]]></addr-line>
<country>Colombia</country>
</aff>
<pub-date pub-type="pub">
<day>00</day>
<month>04</month>
<year>2017</year>
</pub-date>
<pub-date pub-type="epub">
<day>00</day>
<month>04</month>
<year>2017</year>
</pub-date>
<volume>46</volume>
<numero>1</numero>
<fpage>60</fpage>
<lpage>68</lpage>
<copyright-statement/>
<copyright-year/>
<self-uri xlink:href="http://www.scielo.org.co/scielo.php?script=sci_arttext&amp;pid=S0120-28042017000100060&amp;lng=en&amp;nrm=iso"></self-uri><self-uri xlink:href="http://www.scielo.org.co/scielo.php?script=sci_abstract&amp;pid=S0120-28042017000100060&amp;lng=en&amp;nrm=iso"></self-uri><self-uri xlink:href="http://www.scielo.org.co/scielo.php?script=sci_pdf&amp;pid=S0120-28042017000100060&amp;lng=en&amp;nrm=iso"></self-uri><abstract abstract-type="short" xml:lang="es"><p><![CDATA[Resumen Se estudiaron cinco variaciones del procedimiento de síntesis de monetita modificando la agitación, la velocidad de adición de acido fosfórico, la homogenización y la temperatura de secado. Los productos se caracterizaron por difracción de rayos X (DRX), microscopia electrónica de barrido (SEM-EDS), relación Ca/P (por titulación de calcio con permanganato de potasio y valoración colorimétrica de fósforo por la formación del complejo azul de molibdeno) y espectroscopia infrarroja con transformada de Fourier (FTIR). Los resultados de DRX, espectroscopia infrarroja y la relación Ca/P señalan que el fosfato sintetizado corresponde a monetita pura. Se encontró que los factores de síntesis que más afectan las propiedades de composición, estructura cristalina, relación Ca/P y forma y tamaño de grano de los fosfatos sintetizados son la relación estequiométrica de los reactantes y la mecanoactivación de sólido con sobrenadante.]]></p></abstract>
<abstract abstract-type="short" xml:lang="en"><p><![CDATA[Abstract Five variations of the monetite (M) synthesis were evaluated modifying the stirring, the phosphoric acid addition rate, the homogeneity and the drying temperature. Products were assessed by means of XRD, FTIR, SEM-EDS analysis and chemical assay of Ca/P (calcium by titration with potassium permanganate and phosphorus by colorimetric assessment of the molybdenum blue complex). X-ray diffraction, infrared spectroscopy and Ca/P ratio indicate that the synthesized phosphate corresponds to pure monetite. It was found that the most influential factors affecting grain composition, crystal size, shape and structure as well as Ca/P molar ratio of synthesized phosphates were stoichiometry and ballmilling mechanoactivation.]]></p></abstract>
<abstract abstract-type="short" xml:lang="pt"><p><![CDATA[Resumo Foram estudadas cinco variações do método de síntese de monetita (M) modificando a agitação, a velocidade de adicáo do acido fosfórico, a homogeneização e a temperatura de secagem. Os produtos foram caracterizados por difratometria de raios X (DRX), microscopia eletrônica de varredura (SEM-EDS), relação Ca/P (Titulação de cálcio com permanganatode potassio e titulação de fósforo pela avaliação colorimetrica do complexo azul de molibdenio), e espectrometria no infra-vermelho com transformada de Fourier (FTIR). Os resultados de DRX, FTIR e relação Ca/P indicam que o fosfato sintetizado corresponde a monetita pura. Foi encontrado que os fatores de sintese que mais afeitam as propriedades da composição, estrutura cristalina, relação Ca/P e a forma e tamanho de grão dos fosfatos sintetizados são a proporção estequiométrica e a mecânoativação do solido com o sobrenadante.]]></p></abstract>
<kwd-group>
<kwd lng="es"><![CDATA[monetita]]></kwd>
<kwd lng="es"><![CDATA[brushita]]></kwd>
<kwd lng="es"><![CDATA[DCPA]]></kwd>
<kwd lng="es"><![CDATA[fosfatos de calcio]]></kwd>
<kwd lng="es"><![CDATA[DCPD]]></kwd>
<kwd lng="es"><![CDATA[hidroxiapatita]]></kwd>
<kwd lng="es"><![CDATA[síntesis de fosfatos]]></kwd>
<kwd lng="en"><![CDATA[monetite]]></kwd>
<kwd lng="en"><![CDATA[brushite]]></kwd>
<kwd lng="en"><![CDATA[DCPA]]></kwd>
<kwd lng="en"><![CDATA[calcium phosphates]]></kwd>
<kwd lng="en"><![CDATA[DCPD]]></kwd>
<kwd lng="en"><![CDATA[hydroxyapatite]]></kwd>
<kwd lng="en"><![CDATA[phosphates synthesis]]></kwd>
<kwd lng="pt"><![CDATA[monetita]]></kwd>
<kwd lng="pt"><![CDATA[brushita]]></kwd>
<kwd lng="pt"><![CDATA[DCPA]]></kwd>
<kwd lng="pt"><![CDATA[fosfatos de cálcio]]></kwd>
<kwd lng="pt"><![CDATA[DCPD]]></kwd>
<kwd lng="pt"><![CDATA[hidroxiapatita]]></kwd>
<kwd lng="pt"><![CDATA[síntese de fosfatos]]></kwd>
</kwd-group>
</article-meta>
</front><back>
<ref-list>
<ref id="B1">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Calcium orthophosphate (CaP04): occurrence and properties]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Dorozhkin]]></surname>
<given-names><![CDATA[S.V]]></given-names>
</name>
</person-group>
<source><![CDATA[Prog. biomater]]></source>
<year>2016</year>
<volume>5</volume>
<page-range>9-70</page-range></nlm-citation>
</ref>
<ref id="B2">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Dicalcium phosphate cements: Brushite and monetite]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Tamimi]]></surname>
<given-names><![CDATA[F.]]></given-names>
</name>
<name>
<surname><![CDATA[Sheikh]]></surname>
<given-names><![CDATA[Z.]]></given-names>
</name>
<name>
<surname><![CDATA[Barralet]]></surname>
<given-names><![CDATA[J]]></given-names>
</name>
</person-group>
<source><![CDATA[Acta Biomater]]></source>
<year>2012</year>
<volume>8</volume>
<page-range>474-87</page-range></nlm-citation>
</ref>
<ref id="B3">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Biological and medical significance of calcium phosphates]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Sergey]]></surname>
<given-names><![CDATA[V]]></given-names>
</name>
<name>
<surname><![CDATA[Matthias]]></surname>
<given-names><![CDATA[E]]></given-names>
</name>
</person-group>
<source><![CDATA[Angew. Chem., Int. Ed]]></source>
<year>2002</year>
<volume>41</volume>
<page-range>3130-46</page-range></nlm-citation>
</ref>
<ref id="B4">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Factors influencing calcium phosphate cement shelf-life]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Gbureck]]></surname>
<given-names><![CDATA[U.]]></given-names>
</name>
<name>
<surname><![CDATA[Dembski]]></surname>
<given-names><![CDATA[S.]]></given-names>
</name>
<name>
<surname><![CDATA[Thull]]></surname>
<given-names><![CDATA[R.]]></given-names>
</name>
<name>
<surname><![CDATA[Barralet]]></surname>
<given-names><![CDATA[J.E]]></given-names>
</name>
</person-group>
<source><![CDATA[Biomaterials]]></source>
<year>2005</year>
<volume>26</volume>
<page-range>3691-7</page-range></nlm-citation>
</ref>
<ref id="B5">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Biomimetic deposition of hydroxyapatite on brushite single crystals grown by the gel technique]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Kumar]]></surname>
<given-names><![CDATA[R.R.]]></given-names>
</name>
<name>
<surname><![CDATA[Wang]]></surname>
<given-names><![CDATA[M]]></given-names>
</name>
</person-group>
<source><![CDATA[Mater. Lett]]></source>
<year>2001</year>
<volume>49</volume>
<page-range>15-9</page-range></nlm-citation>
</ref>
<ref id="B6">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Mechanical characterization of brushite and hydro yapatite cements]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Charriere]]></surname>
<given-names><![CDATA[E.]]></given-names>
</name>
<name>
<surname><![CDATA[Terrazzoni]]></surname>
<given-names><![CDATA[S]]></given-names>
</name>
<name>
<surname><![CDATA[Pittet]]></surname>
<given-names><![CDATA[C]]></given-names>
</name>
<name>
<surname><![CDATA[Mordasini]]></surname>
<given-names><![CDATA[P.H.]]></given-names>
</name>
<name>
<surname><![CDATA[Dutoit]]></surname>
<given-names><![CDATA[M.]]></given-names>
</name>
<name>
<surname><![CDATA[Lemaitre]]></surname>
<given-names><![CDATA[J.]]></given-names>
</name>
</person-group>
<source><![CDATA[Biomaterials]]></source>
<year>2001</year>
<volume>22</volume>
<page-range>2937-645</page-range></nlm-citation>
</ref>
<ref id="B7">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Biocompatibility and resorption of a brushite calcium phosphate cement]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Theiss]]></surname>
<given-names><![CDATA[F.]]></given-names>
</name>
<name>
<surname><![CDATA[Apelt]]></surname>
<given-names><![CDATA[D.]]></given-names>
</name>
<name>
<surname><![CDATA[Brand]]></surname>
<given-names><![CDATA[B.]]></given-names>
</name>
<name>
<surname><![CDATA[Kutter]]></surname>
<given-names><![CDATA[A.]]></given-names>
</name>
<name>
<surname><![CDATA[Zlinszky]]></surname>
<given-names><![CDATA[K.]]></given-names>
</name>
<name>
<surname><![CDATA[Bohner]]></surname>
<given-names><![CDATA[M.]]></given-names>
</name>
</person-group>
<source><![CDATA[Biomaterials]]></source>
<year>2005</year>
<volume>26</volume>
<page-range>4383-94</page-range></nlm-citation>
</ref>
<ref id="B8">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[New knowledge of chondrocalcinosis]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Dieppe]]></surname>
<given-names><![CDATA[P]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Clin. Pathol]]></source>
<year>1978</year>
<volume>31</volume>
<numero>^s12</numero>
<issue>^s12</issue>
<supplement>12</supplement>
<page-range>214-22</page-range></nlm-citation>
</ref>
<ref id="B9">
<nlm-citation citation-type="">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Dorozhikin]]></surname>
<given-names><![CDATA[S.V]]></given-names>
</name>
</person-group>
<article-title xml:lang=""><![CDATA[Calcium orthophopsphates as biomterials and bioceramics En: Bioceramics properties, preparation and applications]]></article-title>
<person-group person-group-type="editor">
<name>
<surname><![CDATA[Kossler]]></surname>
<given-names><![CDATA[W.]]></given-names>
</name>
<name>
<surname><![CDATA[Fuchs]]></surname>
<given-names><![CDATA[J]]></given-names>
</name>
</person-group>
<source><![CDATA[Nova Biomedical Books]]></source>
<year>2009</year>
<page-range>73</page-range><publisher-loc><![CDATA[New York ]]></publisher-loc>
</nlm-citation>
</ref>
<ref id="B10">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[De Aza]]></surname>
<given-names><![CDATA[P.N.]]></given-names>
</name>
<name>
<surname><![CDATA[De Aza]]></surname>
<given-names><![CDATA[S]]></given-names>
</name>
</person-group>
<article-title xml:lang=""><![CDATA[Biocerámicas]]></article-title>
<person-group person-group-type="editor">
<name>
<surname><![CDATA[Sastre]]></surname>
<given-names><![CDATA[R.]]></given-names>
</name>
<name>
<surname><![CDATA[De Aza]]></surname>
<given-names><![CDATA[S.]]></given-names>
</name>
<name>
<surname><![CDATA[San Roman]]></surname>
<given-names><![CDATA[J]]></given-names>
</name>
</person-group>
<source><![CDATA[Biomaterials]]></source>
<year>2004</year>
<page-range>55</page-range><publisher-loc><![CDATA[Faenza (Italia) ]]></publisher-loc>
<publisher-name><![CDATA[Litográfica Faenza]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B11">
<nlm-citation citation-type="book">
<article-title xml:lang=""><![CDATA[Phosphorus]]></article-title>
<collab>Corbridge, D E C</collab>
<source><![CDATA[Studies in inorganic chemistry]]></source>
<year>1995</year>
<volume>20</volume>
<page-range>169-305</page-range><publisher-name><![CDATA[Elsevier Science B.V]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B12">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Effects of magnesium on calcium phosphate formation]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Cheng]]></surname>
<given-names><![CDATA[P T]]></given-names>
</name>
<name>
<surname><![CDATA[Grabher]]></surname>
<given-names><![CDATA[J J]]></given-names>
</name>
<name>
<surname><![CDATA[LeGeros]]></surname>
<given-names><![CDATA[R Z]]></given-names>
</name>
</person-group>
<source><![CDATA[Magnesium]]></source>
<year>1988</year>
<volume>7</volume>
<page-range>123-32</page-range></nlm-citation>
</ref>
<ref id="B13">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Lundager Madsen]]></surname>
<given-names><![CDATA[H.E.]]></given-names>
</name>
<name>
<surname><![CDATA[Pedersen]]></surname>
<given-names><![CDATA[J.B]]></given-names>
</name>
</person-group>
<article-title xml:lang=""><![CDATA[Influence of foreign metal ions on crystal morphology and transformation of brushite (CaHP04.2H20)]]></article-title>
<person-group person-group-type="editor">
<name>
<surname><![CDATA[Amjad]]></surname>
<given-names><![CDATA[Z]]></given-names>
</name>
</person-group>
<source><![CDATA[Advances in crystal growth inhibition technologies]]></source>
<year>2000</year>
<page-range>1</page-range><publisher-loc><![CDATA[New York ]]></publisher-loc>
<publisher-name><![CDATA[Kluwer Academic/Plenum Publishers]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B14">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Monetite promoting effect of NaCl on brushite cement setting kinetics]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Sahin]]></surname>
<given-names><![CDATA[E.]]></given-names>
</name>
<name>
<surname><![CDATA[Ciftcioglu]]></surname>
<given-names><![CDATA[M]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Mater. Chem. B]]></source>
<year>2013</year>
<volume>1</volume>
<page-range>2943-50</page-range></nlm-citation>
</ref>
<ref id="B15">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Role of Strontium on the Crystallization of Calcium Hydrogen Phosphate Dihydrate (CHPD)]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Suguna]]></surname>
<given-names><![CDATA[K]]></given-names>
</name>
<name>
<surname><![CDATA[Sekar]]></surname>
<given-names><![CDATA[C]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Miner. Mater. Charact. Eng]]></source>
<year>2011</year>
<volume>10</volume>
<page-range>625-36</page-range></nlm-citation>
</ref>
<ref id="B16">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Influence of an organic and an inorganic additive on the crystallization of dicalcium phosphate dehydrate]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Anee]]></surname>
<given-names><![CDATA[T K]]></given-names>
</name>
<name>
<surname><![CDATA[Meenakshi]]></surname>
<given-names><![CDATA[S N]]></given-names>
</name>
<name>
<surname><![CDATA[Arivuoli]]></surname>
<given-names><![CDATA[D]]></given-names>
</name>
<name>
<surname><![CDATA[Ramasamy]]></surname>
<given-names><![CDATA[P]]></given-names>
</name>
<name>
<surname><![CDATA[Kalkura]]></surname>
<given-names><![CDATA[N S]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Cryst. Growth]]></source>
<year>2005</year>
<volume>285</volume>
<page-range>380-7</page-range></nlm-citation>
</ref>
<ref id="B17">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Mineralization of calcium phosphate in reverse microemulsion]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Xian]]></surname>
<given-names><![CDATA[D. K.]]></given-names>
</name>
<name>
<surname><![CDATA[Xiao]]></surname>
<given-names><![CDATA[D. S.]]></given-names>
</name>
<name>
<surname><![CDATA[Jun]]></surname>
<given-names><![CDATA[B. L.]]></given-names>
</name>
<name>
<surname><![CDATA[Fu]]></surname>
<given-names><![CDATA[C]]></given-names>
</name>
</person-group>
<source><![CDATA[Curr. Appl. Phys]]></source>
<year>2005</year>
<volume>5</volume>
<page-range>519-21</page-range></nlm-citation>
</ref>
<ref id="B18">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Ruiz]]></surname>
<given-names><![CDATA[S C]]></given-names>
</name>
</person-group>
<source><![CDATA[Propuesta y evaluación de una síntesis rápida y selectiva de algunos fosfatos de calcio por el método ácido-base]]></source>
<year>2005</year>
<publisher-loc><![CDATA[Bogotá, D C, Colombia ]]></publisher-loc>
<publisher-name><![CDATA[Universidad Nacional de Colombia]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B19">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Controllability of brushite structural parameters using an applied magnetic field]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Kuznetsov]]></surname>
<given-names><![CDATA[V N]]></given-names>
</name>
<name>
<surname><![CDATA[Yanovska]]></surname>
<given-names><![CDATA[A A]]></given-names>
</name>
<name>
<surname><![CDATA[Stanislavov]]></surname>
<given-names><![CDATA[A S]]></given-names>
</name>
<name>
<surname><![CDATA[Danilchenkoa]]></surname>
<given-names><![CDATA[S.N.]]></given-names>
</name>
<name>
<surname><![CDATA[Kalinkevich]]></surname>
<given-names><![CDATA[A.N.]]></given-names>
</name>
<name>
<surname><![CDATA[Sukhodub]]></surname>
<given-names><![CDATA[L.F]]></given-names>
</name>
</person-group>
<source><![CDATA[Mater. Sc. Eng. C]]></source>
<year>2016</year>
<volume>60</volume>
<page-range>547-53</page-range></nlm-citation>
</ref>
<ref id="B20">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Experimental study of brushite precipitation]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Arifuzzaman]]></surname>
<given-names><![CDATA[S M]]></given-names>
</name>
<name>
<surname><![CDATA[Rohani]]></surname>
<given-names><![CDATA[S]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Cryst Growth]]></source>
<year>2004</year>
<volume>267</volume>
<page-range>624-34</page-range></nlm-citation>
</ref>
<ref id="B21">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[The role of the chemical composition of monetite on the synthesis and properties of a-tricalcium phosphate]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Duncan]]></surname>
<given-names><![CDATA[J.]]></given-names>
</name>
<name>
<surname><![CDATA[MacDonald]]></surname>
<given-names><![CDATA[J F.]]></given-names>
</name>
<name>
<surname><![CDATA[Hanna]]></surname>
<given-names><![CDATA[J V.]]></given-names>
</name>
<name>
<surname><![CDATA[Shirosaki]]></surname>
<given-names><![CDATA[Y.]]></given-names>
</name>
<name>
<surname><![CDATA[Hayakawa]]></surname>
<given-names><![CDATA[S.]]></given-names>
</name>
<name>
<surname><![CDATA[Osaka]]></surname>
<given-names><![CDATA[A.]]></given-names>
</name>
<name>
<surname><![CDATA[Skakle]]></surname>
<given-names><![CDATA[J.M.S.]]></given-names>
</name>
<name>
<surname><![CDATA[Gibson]]></surname>
<given-names><![CDATA[I. R]]></given-names>
</name>
</person-group>
<source><![CDATA[Mater. Sci. Eng. C]]></source>
<year>2014</year>
<volume>34</volume>
<page-range>123-9</page-range></nlm-citation>
</ref>
<ref id="B22">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Synthesis and characterization of nanocomposite based on hydro yapatite and monetite]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Higuita]]></surname>
<given-names><![CDATA[L. P.]]></given-names>
</name>
<name>
<surname><![CDATA[Vargas]]></surname>
<given-names><![CDATA[A. F.]]></given-names>
</name>
<name>
<surname><![CDATA[Gil]]></surname>
<given-names><![CDATA[M. J.]]></given-names>
</name>
<name>
<surname><![CDATA[Giraldo]]></surname>
<given-names><![CDATA[L. F]]></given-names>
</name>
</person-group>
<source><![CDATA[Mater. Lett]]></source>
<year>2016</year>
<volume>175</volume>
<page-range>169-72</page-range></nlm-citation>
</ref>
<ref id="B23">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Thermal decomposition of brushite CaHPO4 2H2O to monetite CaHPO4 and the formation of an amorphous phase]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Dosen]]></surname>
<given-names><![CDATA[A]]></given-names>
</name>
<name>
<surname><![CDATA[Giese]]></surname>
<given-names><![CDATA[R F]]></given-names>
</name>
</person-group>
<source><![CDATA[Am. Mineralogist]]></source>
<year>2011</year>
<volume>96</volume>
<page-range>368-73</page-range></nlm-citation>
</ref>
<ref id="B24">
<nlm-citation citation-type="">
<source><![CDATA[Selected solubility products and formation constants]]></source>
<year></year>
</nlm-citation>
</ref>
<ref id="B25">
<nlm-citation citation-type="">
<source><![CDATA[Venter, A.C. U.S. Patent WO2012176151A1]]></source>
<year>2012</year>
</nlm-citation>
</ref>
<ref id="B26">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Calcium orthophosphates Occurrence, properties, biomineralization, pathological calcification and biomimetic applications]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Dorozhkin]]></surname>
<given-names><![CDATA[S]]></given-names>
</name>
</person-group>
<source><![CDATA[Biomatter]]></source>
<year>2011</year>
<volume>1</volume>
<page-range>121-64</page-range></nlm-citation>
</ref>
<ref id="B27">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[A single solution method for the determination of soluble phosphate in sea water]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Murphy J]]></surname>
<given-names><![CDATA[Riley J P]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Mar. Biol. Assoc]]></source>
<year>1958</year>
<volume>37</volume>
<page-range>9-14</page-range></nlm-citation>
</ref>
<ref id="B28">
<nlm-citation citation-type="">
<source><![CDATA[ISO 8556 Aluminium ores - Determination of phosphorus content -Molybdenum blue spectrophotometry method]]></source>
<year>1984</year>
<month>z</month>
</nlm-citation>
</ref>
<ref id="B29">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[PowderX: Windows-95-based program for powder X-ray diffraction data processing]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Dong]]></surname>
<given-names><![CDATA[C]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Appl. Cryst]]></source>
<year>1999</year>
<volume>32</volume>
<page-range>838</page-range></nlm-citation>
</ref>
<ref id="B30">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Abridged acid-base wet-milling synthesis of high purity hydroxyapatite]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Ruiz]]></surname>
<given-names><![CDATA[S.C.]]></given-names>
</name>
<name>
<surname><![CDATA[Moreno]]></surname>
<given-names><![CDATA[L.C.]]></given-names>
</name>
<name>
<surname><![CDATA[Delgado]]></surname>
<given-names><![CDATA[E]]></given-names>
</name>
</person-group>
<source><![CDATA[Mater. Res]]></source>
<year>2008</year>
<volume>11</volume>
<page-range>187-92</page-range></nlm-citation>
</ref>
<ref id="B31">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Electrochemical synthesis of nanosi ed monetite powder and its electrophoretic deposition on titanium]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Djosic]]></surname>
<given-names><![CDATA[M.S.]]></given-names>
</name>
<name>
<surname><![CDATA[Miskovic-Stankovic]]></surname>
<given-names><![CDATA[V.B.]]></given-names>
</name>
<name>
<surname><![CDATA[Kacarevic-Popovic]]></surname>
<given-names><![CDATA[Z. M.]]></given-names>
</name>
<name>
<surname><![CDATA[Jokic]]></surname>
<given-names><![CDATA[B.M.]]></given-names>
</name>
<name>
<surname><![CDATA[Bibic]]></surname>
<given-names><![CDATA[N.]]></given-names>
</name>
<name>
<surname><![CDATA[Mitric]]></surname>
<given-names><![CDATA[M.]]></given-names>
</name>
</person-group>
<source><![CDATA[Colloids Surf., A]]></source>
<year>2009</year>
<volume>341</volume>
<page-range>110-7</page-range></nlm-citation>
</ref>
<ref id="B32">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[Study of protonic mobility in CaHPO4*2H2O (brushite) and CaHPO4 (monetite) by infrared spectroscopy and neutron scattering]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Tortet]]></surname>
<given-names><![CDATA[L.]]></given-names>
</name>
<name>
<surname><![CDATA[Gavarri]]></surname>
<given-names><![CDATA[J. R]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Solid State Chem]]></source>
<year>1997</year>
<volume>132</volume>
<page-range>6-16</page-range></nlm-citation>
</ref>
<ref id="B33">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[FT-Raman and high-pressure infrared spectroscopic studies of dicalcium phosphate dehydrate (CaHPO4*2H2O) and anhydrous dicalcium phosphate (CaHPO4)]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Jingwei]]></surname>
<given-names><![CDATA[X.]]></given-names>
</name>
<name>
<surname><![CDATA[Ian]]></surname>
<given-names><![CDATA[B.S.]]></given-names>
</name>
<name>
<surname><![CDATA[Gilson]]></surname>
<given-names><![CDATA[ER]]></given-names>
</name>
</person-group>
<source><![CDATA[Spectrochim. Acta. Part A]]></source>
<year>1999</year>
<volume>55</volume>
<page-range>2801-9</page-range></nlm-citation>
</ref>
<ref id="B34">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[FTIR reinvestigation of the spectra of synthetic brushite and its partially deuterated analogues]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Trpkovska]]></surname>
<given-names><![CDATA[M.]]></given-names>
</name>
<name>
<surname><![CDATA[Bojan]]></surname>
<given-names><![CDATA[S.]]></given-names>
</name>
<name>
<surname><![CDATA[Pavle]]></surname>
<given-names><![CDATA[M]]></given-names>
</name>
</person-group>
<source><![CDATA[J. Mol. Struct]]></source>
<year>1999</year>
<volume>480-481</volume>
<page-range>661-6</page-range></nlm-citation>
</ref>
<ref id="B35">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Elliot]]></surname>
<given-names><![CDATA[J.C]]></given-names>
</name>
</person-group>
<source><![CDATA[Structure and chemistry of the apatites and other calcium orthophosphates]]></source>
<year>1994</year>
<page-range>305-10</page-range><publisher-loc><![CDATA[Amsterdam, London ]]></publisher-loc>
<publisher-name><![CDATA[Elsevier]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B36">
<nlm-citation citation-type="journal">
<article-title xml:lang=""><![CDATA[XRD, AFM, IR and TGA Study of Nanostructured Hydroxyapatite]]></article-title>
<person-group person-group-type="author">
<name>
<surname><![CDATA[Mir]]></surname>
<given-names><![CDATA[M.]]></given-names>
</name>
<name>
<surname><![CDATA[Leiteb]]></surname>
<given-names><![CDATA[F.L.]]></given-names>
</name>
<name>
<surname><![CDATA[Herrmann Junior]]></surname>
<given-names><![CDATA[P.S.P.]]></given-names>
</name>
<name>
<surname><![CDATA[Pissetti]]></surname>
<given-names><![CDATA[F.L.]]></given-names>
</name>
<name>
<surname><![CDATA[Malta Rossi]]></surname>
<given-names><![CDATA[A]]></given-names>
</name>
<name>
<surname><![CDATA[Lima Moreira]]></surname>
<given-names><![CDATA[E]]></given-names>
</name>
</person-group>
<source><![CDATA[Mater. Res]]></source>
<year>2012</year>
<volume>15</volume>
<page-range>622-7</page-range></nlm-citation>
</ref>
</ref-list>
</back>
</article>
