<?xml version="1.0" encoding="ISO-8859-1"?><article xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance">
<front>
<journal-meta>
<journal-id>1794-1237</journal-id>
<journal-title><![CDATA[Revista EIA]]></journal-title>
<abbrev-journal-title><![CDATA[Rev.EIA.Esc.Ing.Antioq]]></abbrev-journal-title>
<issn>1794-1237</issn>
<publisher>
<publisher-name><![CDATA[Escuela de ingenieria de Antioquia]]></publisher-name>
</publisher>
</journal-meta>
<article-meta>
<article-id>S1794-12372012000100016</article-id>
<title-group>
<article-title xml:lang="en"><![CDATA[EVALUATION OF HMA CRACKING RESISTANCE AS A FUNCTION OF LABORATORY AGING BASED ON THE DIRECT-TENSION TEST]]></article-title>
<article-title xml:lang="es"><![CDATA[EVALUACIÓN DE LA RESISTENCIA AL AGRIETAMIENTO DE MEZCLAS ASFÁLTICAS EN CALIENTE EN FUNCIÓN DE SU ENVEJECIMIENTO A PARTIR DEL ENSAYO DE TENSIÓN DIRECTA]]></article-title>
<article-title xml:lang="pt"><![CDATA[AVALIAÇÃO DA RESISTÊNCIA AS RACHADURAS DE MISTURAS ASFÁLTICAS EM QUENTE EM FUNÇÃO DE SEU ENVELHECIMENTO A PARTIR DO ENSAIO DE TENSÃO DIRETA]]></article-title>
</title-group>
<contrib-group>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Walubita]]></surname>
<given-names><![CDATA[Lubinda F]]></given-names>
</name>
<xref ref-type="aff" rid="A01"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Flórez]]></surname>
<given-names><![CDATA[Blanca L]]></given-names>
</name>
<xref ref-type="aff" rid="A02"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Álvarez]]></surname>
<given-names><![CDATA[Allex E]]></given-names>
</name>
<xref ref-type="aff" rid="A03"/>
</contrib>
</contrib-group>
<aff id="A01">
<institution><![CDATA[,Texas Transportation Institute-TTI  ]]></institution>
<addr-line><![CDATA[College Station TX]]></addr-line>
<country>USA</country>
</aff>
<aff id="A02">
<institution><![CDATA[,Universidad del Magdalena Grupo Integrado de Investigación en Ingeniería Civil (GIIC) ]]></institution>
<addr-line><![CDATA[Santa Marta ]]></addr-line>
<country>Colombia</country>
</aff>
<aff id="A03">
<institution><![CDATA[,Universidad del Magdalena Grupo Integrado de Investigación en Ingeniería Civil (GIIC) ]]></institution>
<addr-line><![CDATA[Santa Marta ]]></addr-line>
<country>Colombia</country>
</aff>
<pub-date pub-type="pub">
<day>00</day>
<month>06</month>
<year>2012</year>
</pub-date>
<pub-date pub-type="epub">
<day>00</day>
<month>06</month>
<year>2012</year>
</pub-date>
<numero>17</numero>
<fpage>209</fpage>
<lpage>224</lpage>
<copyright-statement/>
<copyright-year/>
<self-uri xlink:href="http://www.scielo.org.co/scielo.php?script=sci_arttext&amp;pid=S1794-12372012000100016&amp;lng=en&amp;nrm=iso"></self-uri><self-uri xlink:href="http://www.scielo.org.co/scielo.php?script=sci_abstract&amp;pid=S1794-12372012000100016&amp;lng=en&amp;nrm=iso"></self-uri><self-uri xlink:href="http://www.scielo.org.co/scielo.php?script=sci_pdf&amp;pid=S1794-12372012000100016&amp;lng=en&amp;nrm=iso"></self-uri><abstract abstract-type="short" xml:lang="en"><p><![CDATA[Hot mix asphalt (HMA) is a heterogeneous composite material of asphalt-binder, aggregates, air voids, and other additives including lime, fibers, etc., predominantly used for pavement construction. With time, the HMA mix ages, which leads to changes in the material properties and response behavior. This paper documents a laboratory study that was conducted to evaluate the suitability of the direct-tension (DT) test to assess the effects of asphalt-binder aging on the HMA mix fracture properties and cracking-resistance potential. Two dense-graded HMA mixes were subjected to different laboratory aging exposure conditions and then tested with the DT test. From this test, the HMA mix fracture response was characterized in terms of the tensile strength, tensile strain at peak failure load, stiffness, and fracture energy. Overall, the results indicated that asphalt-binder aging has a detrimental effect on the fracture response and cracking-resistance of HMA mixes, which can be captured based on the DT test. Therefore, the asphalt-binder aging needs to be considered and properly accounted for during the material design and analysis stages of HMA mixes. However, research with more HMA mixes and correlation with field data is strongly recommended to validate the laboratory findings reported in this paper.]]></p></abstract>
<abstract abstract-type="short" xml:lang="es"><p><![CDATA[La mezcla asfáltica en caliente (MAC) es un material compuesto, heterogéneo, integrado por cemento asfáltico (o asfalto), agregados, vacíos y otros aditivos incluyendo cal, fibras, etc., usado predominantemente para la construcción de pavimentos. A lo largo del tiempo, la MAC sufre envejecimiento, lo cual conlleva cambios en las propiedades del material y en su respuesta. Este artículo documenta un estudio de laboratorio llevado a cabo para evaluar la posibilidad de emplear el ensayo de tensión directa (TD) para determinar los efectos del envejecimiento del asfalto sobre las propiedades de fractura y resistencia al agrietamiento de MAC. Dos MAC de gradación densa fueron sometidas a diferentes condiciones de envejecimiento en laboratorio y luego sometidas al ensayo de TD. A partir de este ensayo, el comportamiento ante fractura se caracterizó en términos de la resistencia a tensión, deformación unitaria de tensión a la carga de falla, rigidez y energía de fractura. En general, los resultados indicaron que el envejecimiento por oxidación del asfalto tiene un efecto negativo sobre la respuesta ante fractura y la resistencia al agrietamiento de la MAC, el cual puede ser captado por medio del ensayo de TD. Por lo tanto, el envejecimiento del asfalto debe ser considerado y cuantificado en forma adecuada durante el diseño y análisis de la MAC. Sin embargo, se recomienda adelantar investigación adicional con otras mezclas y correlacionar resultados con datos de campo para validar la información de laboratorio reportada en este artículo.]]></p></abstract>
<abstract abstract-type="short" xml:lang="pt"><p><![CDATA[A mistura asfáltica em quente (MAQ) é um material composto, heterogéneo, integrado por cimento asfáltico (ou asfalto), agregados, vazios e outros aditivos incluindo cal, fibras, etc., usado predominantemente para a construção de pavimentos. Ao longo do tempo, a MAC sofre envelhecimento, o qual implica mudanças nas propriedades do material e em sua resposta. Este artigo documenta um estudo de laboratório levado a cabo para avaliar a possibilidade de empregar o ensaio de tensão direta (TD) para determinar os efeitos do envelhecimento do asfalto sobre as propriedades de fratura e resistência à rachadura de MAC. Dois MAC de gradação densa foram submetidas a diferentes condições de envelhecimento em laboratório e depois submetidas ao ensaio de TD. A partir deste ensaio, o comportamento à fratura caracterizou-se em termos da resistência a tensão, deformação unitária de tensão à carga de falha, rigidez e energia de fratura. Em geral, os resultados indicaram que o envelhecimento por oxidação do asfalto tem um efeito negativo sobre a resposta à fratura e a resistência à rachadura da MAC, o qual pode ser captado através do ensaio de TD. Portanto, o envelhecimento do asfalto deve ser considerado e quantificado em forma adequada durante o desenho e análise da MAC. No entanto, recomenda-se fazer pesquisa adicional com outras misturas e correlacionar resultados com dados de campo para validar a informação de laboratório reportada em este artigo.]]></p></abstract>
<kwd-group>
<kwd lng="en"><![CDATA[asphalt-binder]]></kwd>
<kwd lng="en"><![CDATA[hot mix asphalt (HMA)]]></kwd>
<kwd lng="en"><![CDATA[aging]]></kwd>
<kwd lng="en"><![CDATA[fracture]]></kwd>
<kwd lng="en"><![CDATA[cracking]]></kwd>
<kwd lng="es"><![CDATA[cemento asfáltico]]></kwd>
<kwd lng="es"><![CDATA[mezcla asfáltica en caliente]]></kwd>
<kwd lng="es"><![CDATA[envejecimiento]]></kwd>
<kwd lng="es"><![CDATA[fractura]]></kwd>
<kwd lng="es"><![CDATA[agrietamiento]]></kwd>
<kwd lng="pt"><![CDATA[cimento asfáltico]]></kwd>
<kwd lng="pt"><![CDATA[mistura asfáltica em quente]]></kwd>
<kwd lng="pt"><![CDATA[envelhecimento]]></kwd>
<kwd lng="pt"><![CDATA[fratura]]></kwd>
<kwd lng="pt"><![CDATA[rachadura]]></kwd>
</kwd-group>
</article-meta>
</front><body><![CDATA[  <font face="verdana" size="2">          <p align="center"><font size="4"><b>EVALUATION OF HMA CRACKING RESISTANCE AS A FUNCTION OF LABORATORY AGING BASED ON THE DIRECT-TENSION TEST </b></font></p>     <p align="center"><font size="3"><b>EVALUACI&Oacute;N DE LA RESISTENCIA AL AGRIETAMIENTO DE MEZCLAS ASF&Aacute;LTICAS EN CALIENTE EN FUNCI&Oacute;N DE SU ENVEJECIMIENTO A PARTIR DEL ENSAYO DE TENSI&Oacute;N DIRECTA </b></font></p>     <p align="center"><font size="3"><b>AVALIA&Ccedil;&Atilde;O DA RESIST&Ecirc;NCIA AS RACHADURAS DE MISTURAS ASF&Aacute;LTICAS EM QUENTE EM FUN&Ccedil;&Atilde;O DE SEU ENVELHECIMENTO A PARTIR DO ENSAIO DE TENS&Atilde;O DIRETA </b></font></p>     <p>&nbsp;</p>     <p><b>Lubinda F. Walubita*, Blanca L. Fl&oacute;rez**, Allex E. &Aacute;lvarez***</b></p>          <p>*Civil Engineer, University of Zambia; M.Sc., Universidad de Stellenbosch; Ph.D., Texas A and M University. Researcher, Texas Transportation Institute-TTI, The Texas A and M University System. College Station, TX, USA. <a href="mailto:l-walubita@ttimail.tamu.edu">l-walubita@ttimail.tamu.edu</a>.    <br>   **Ingeniera Civil y Miembro del Grupo Integrado de Investigaci&oacute;n en Ingenier&iacute;a Civil (GIIC), Universidad del Magdalena. Santa Marta, Colombia. <a href="mailto:elvica-25@hotmail.com">elvica-25@hotmail.com</a>.    <br> ***Ingeniero Civil, Universidad Nacional de Colombia; M.Sc., Universidad de los Andes, Bogot&aacute;; Ph.D., Texas A and M University. Profesor Asociado y Director del Grupo Integrado de Investigaci&oacute;n en Ingenier&iacute;a Civil (GIIC), Universidad del Magdalena. Santa Marta, Colombia. <a href="mailto:aalvarez@unimagdalena.edu.co">aalvarez@unimagdalena.edu.co</a>.</p>     <p>Art&iacute;culo recibido 31-VIII-2011. Aprobado 19-VI-2012    ]]></body>
<body><![CDATA[<br> Discusi&oacute;n abierta hasta diciembre de 2012</p> <hr size="1" />              <p><b><font size="3">ABSTRACT</font></b></p>          <p>Hot mix asphalt (HMA) is a heterogeneous composite material of asphalt-binder, aggregates, air voids, and other additives including lime, fibers, etc., predominantly used for pavement construction. With time, the HMA mix ages, which leads to changes in the material properties and response behavior. This paper documents a laboratory study that was conducted to evaluate the suitability of the direct-tension (DT) test to assess the effects of asphalt-binder aging on the HMA mix fracture properties and cracking-resistance potential. Two dense-graded HMA mixes were subjected to different laboratory aging exposure conditions and then tested with the DT test. From this test, the HMA mix fracture response was characterized in terms of the tensile strength, tensile strain at peak failure load, stiffness, and fracture energy. Overall, the results indicated that asphalt-binder aging has a detrimental effect on the fracture response and cracking-resistance of HMA mixes, which can be captured based on the DT test. Therefore, the asphalt-binder aging needs to be considered and properly accounted for during the material design and analysis stages of HMA mixes. However, research with more HMA mixes and correlation with field data is strongly recommended to validate the laboratory findings reported in this paper.</p>          <p><font size="3"><b>KEY WORDS</b></font>: asphalt-binder; hot mix asphalt (HMA); aging; fracture; cracking.</p>  <hr size="1" />              <p><font size="3"><b>RESUMEN</b></font></p>          <p>La mezcla asf&aacute;ltica en caliente (MAC) es un material compuesto, heterog&eacute;neo, integrado por cemento asf&aacute;ltico (o asfalto), agregados, vac&iacute;os y otros aditivos incluyendo cal, fibras, etc., usado predominantemente para la construcci&oacute;n de pavimentos. A lo largo del tiempo, la MAC sufre envejecimiento, lo cual conlleva cambios en las propiedades del material y en su respuesta. Este art&iacute;culo documenta un estudio de laboratorio llevado a cabo para evaluar la posibilidad de emplear el ensayo de tensi&oacute;n directa (TD) para determinar los efectos del envejecimiento del asfalto sobre las propiedades de fractura y resistencia al agrietamiento de MAC. Dos MAC de gradaci&oacute;n densa fueron sometidas a diferentes condiciones de envejecimiento en laboratorio y luego sometidas al ensayo de TD. A partir de este ensayo, el comportamiento ante fractura se caracteriz&oacute; en t&eacute;rminos de la resistencia a tensi&oacute;n, deformaci&oacute;n unitaria de tensi&oacute;n a la carga de falla, rigidez y energ&iacute;a de fractura. En general, los resultados indicaron que el envejecimiento por oxidaci&oacute;n del asfalto tiene un efecto negativo sobre la respuesta ante fractura y la resistencia al agrietamiento de la MAC, el cual puede ser captado por medio del ensayo de TD. Por lo tanto, el envejecimiento del asfalto debe ser considerado y cuantificado en forma adecuada durante el dise&ntilde;o y an&aacute;lisis de la MAC. Sin embargo, se recomienda adelantar investigaci&oacute;n adicional con otras mezclas y correlacionar resultados con datos de campo para validar la informaci&oacute;n de laboratorio reportada en este art&iacute;culo.</p>     <p><font size="3"><b>PALABRAS CLAVE</b></font>: cemento asf&aacute;ltico; mezcla asf&aacute;ltica en caliente; envejecimiento; fractura; agrietamiento.</p>  <hr size="1" />      <p><b><font size="3">RESUMO</font></b></p>          <p>A mistura asf&aacute;ltica em quente (MAQ) &eacute; um material composto, heterog&eacute;neo, integrado por cimento asf&aacute;ltico (ou asfalto), agregados, vazios e outros aditivos incluindo cal, fibras, etc., usado predominantemente para a constru&ccedil;&atilde;o de pavimentos. Ao longo do tempo, a MAC sofre envelhecimento, o qual implica mudan&ccedil;as nas propriedades do material e em sua resposta. Este artigo documenta um estudo de laborat&oacute;rio levado a cabo para avaliar a possibilidade de empregar o ensaio de tens&atilde;o direta (TD) para determinar os efeitos do envelhecimento do asfalto sobre as propriedades de fratura e resist&ecirc;ncia &agrave; rachadura de MAC. Dois MAC de grada&ccedil;&atilde;o densa foram submetidas a diferentes condi&ccedil;&otilde;es de envelhecimento em laborat&oacute;rio e depois submetidas ao ensaio de TD. A partir deste ensaio, o comportamento &agrave; fratura caracterizou-se em termos da resist&ecirc;ncia a tens&atilde;o, deforma&ccedil;&atilde;o unit&aacute;ria de tens&atilde;o &agrave; carga de falha, rigidez e energia de fratura. Em geral, os resultados indicaram que o envelhecimento por oxida&ccedil;&atilde;o do asfalto tem um efeito negativo sobre a resposta &agrave; fratura e a resist&ecirc;ncia &agrave; rachadura da MAC, o qual pode ser captado atrav&eacute;s do ensaio de TD. Portanto, o envelhecimento do asfalto deve ser considerado e quantificado em forma adequada durante o desenho e an&aacute;lise da MAC. No entanto, recomenda-se fazer pesquisa adicional com outras misturas e correlacionar resultados com dados de campo para validar a informa&ccedil;&atilde;o de laborat&oacute;rio reportada em este artigo.</p>          <p><font size="3"><b>PALAVRAS-C&Oacute;DIGO</b></font>: cimento asf&aacute;ltico; mistura asf&aacute;ltica em quente; envelhecimento; fratura; rachadura.</p>  <hr size="1" />             ]]></body>
<body><![CDATA[<p><font size="3"><b>1. INTRODUCTION</b></font></p>          <p>Hot-mix asphalt (HMA) mix is a heterogeneous   complex composite material of air, asphalt-binder,   aggregate, and other additives such as lime, cellulose   fiber, etc., predominantly used for road pavement   construction. Under traffic loading and changing   environmental conditions, the HMA mix exhibit   non-linear viscoelastic-viscoplastic and anisotropic   behavior (Walubita, 2006; Huang <i>et al</i>., 2011). With   time, the HMA mix, and ultimately the asphalt-binder   in it also ages, but with the potential to heal (closure   of micro-fractured or micro-cracked surfaces) during   traffic loading rest periods (Kim, 2009).</p>     <p>As noted above, the asphalt-binder within   the HMA generally experiences aging with time and   under changing environmental conditions, a process   that often involves chemical and structural changes   in the material (Vargas and Reyes, 2010). The aging   phenomenon starts with the HMA mix fabrication   process -short term aging- and progresses in the   field along the pavement service life -long term   aging-. Besides the original chemical composition   and properties of the asphalt-binder, several aspects   define the field rate of aging in the HMA mix. These   aspects can include, for example, the HMA mix air   void content (Glover <i>et al</i>., 2005), asphalt-binder film   thickness coating the aggregate particles (Kandhal   and Chakraborty, 1996), fabrication temperature of   the HMA mix, and temperature conditions where the   HMA mix performs (Glover <i>et al</i>., 2005).</p>     <p>The changes occurring in the asphalt-binder   due to aging lead to changes in the engineering   properties as well -rheological (Lu and Isacsson,   2002), mechanical (Airey, 2003), and thermodynamic   (Kim, 2009)- of the asphalt-binder and, therefore,   of the corresponding HMA mix. Previous research   reported that aging increased the HMA mix stiffness   and reduced its ductility potential, thus increasing the   HMA mix's brittleness and susceptibility to fracture   damage and cracking (Glover <i>et al</i>., 2005). The susceptibility   to moisture damage may also be altered   or even worsened as the asphalt-binder ages in the   HMA mix (Punith <i>et al</i>., 2012).</p>     <p>In addition, according to Jung (2006), asphaltbinder   aging is very critical in the top portion of   surface HMA layers due to direct environmental exposure   and generally decreases with depth. The net   result is often stiffer and brittle or "dry" HMA layers   that are susceptible to fracture damage and cracking.   In fact, one of the predominant causer of top-down   cracking in HMA pavements is hypothesized to   be asphalt-binder aging, resulting in high thermal   stresses in the HMA mix (PI, 2011). Aging also has a   tendency to reduce the cohesiveness, adhesiveness,   and bonding properties of the asphalt-binder, thus   exacerbating other distresses such as fatigue, moisture   damage, etc., which can promote potholing and,   in general, cause loss of durability. Some examples   of age-related HMA pavement damage are shown   in <a href="#fig1">figure 1</a>.</p>       <p align="center"><img src="img/revistas/eia/n17/n17a16fig1.gif"><a name="fig1"></a></p>     <p>Without doubt, these distresses are undesired   and a financial drain on the highway agencies in   terms of maintenance and rehabilitation activities.   Therefore, there is still a need to fully understand   the effects of asphalt-binder aging on the HMA mix   fracture parameters and cracking resistance potential;   and how this could be incorporated in design   models (i.e., including laboratory testing) so as to   minimize aging related damage and optimize the   HMA mix performance.</p>     <p>Based on the above background, the main   goal of this paper was to evaluate the suitability   of the direct-tension (DT) test to assess the effects   of asphalt-binder aging on the HMA mix fracture   properties and cracking-resistance potential. The   research methodology incorporated evaluation of   HMA mix specimens subjected to aging for 0, 3,   and 6 months in the laboratory. Two dense-graded   mixes were subjected to DT testing to characterize   and measure the following fracture parameters in   response to asphalt-binder aging:</p>   <ul type="disc">     <li>HMA mix tensile strength</li>     <li>HMA mix ductility potential based on the tensile   strain at peak failure load</li>     ]]></body>
<body><![CDATA[<li>HMA mix elastic tensile stiffness (or tensile modulus)</li>     <li>HMA mix fracture energy and associated indices</li>     </ul>     <p>With the above objectives, it should be emphasized   here that direct measurement of the actual   degree, extent, and/or quantification of aging was   outside the scope of this study; these details are   documented elsewhere (Glover <i>et al</i>., 2005; Jung,   2006). The primary focus was to assess how the HMA   fracture properties, as measured with the DT test,   changed and varied as a function of the specified aging   period in the laboratory. Secondly, the intent was   to concurrently evaluate if the DT test was sensitive   enough and able to sufficiently capture the changes   in the HMA fracture properties in response to the   specified laboratory aging conditions.</p>     <p>In terms of the paper layout, following this   introduction is a brief discussion of the kinetics of   asphalt-binder aging, followed by a description of the   DT test protocol, data analysis models for computing   the fracture parameters, and the experimental   design plan. Results are then presented and analyzed,   followed by a summary of key findings and recommendations   to conclude the paper.</p>     <p><font size="3"><b>2. THEORY AND KINETICS OF   ASPHALT-BINDER AGING</b></font></p>     <p>Asphalt-binder can simplistically be defined   as a dark-brown to black viscous-cementitious compound,   predominantly composed -as hypothesized   in the classical asphalt chemistry model- of hydrocarbons   that are associated in two main fractional   components termed as asphaltenes and maltenes   (Pfeiffer and Saal, 1940; Arenas, 2005). Asphaltenes   are the polar, high molecular weight, and less soluble   hydrocarbons that constitute about 5 to 25 % by total   weight of the asphalt-binder. The maltenes, on the   other hand, are non-polar or relatively low polar,   lower molecular weight, and soluble hydrocarbons   (Asphalt Rehab, 2012).</p>     <p>At a microstructural level, asphalt-binder is   thus defined as a suspended polar fluid of a continuous   three-dimensional association of polar molecules   (asphaltenes) suspended in a fluid of non-polar or   relatively low-polarity molecules (maltenes), i.e., colloids   of asphaltene micelles suspended in maltenes   (Lin <i>et al</i>., 1996). The adhesion of asphalt-binder to   aggregate is also thought to depend on the polar   attraction between molecules in the asphalt-binder   and the polar surfaces of the aggregates.</p>     <p><font size="3"><b>2.1 Asphalt-binder aging and   embrittlement</b></font></p>     <p>During aging, the asphalt-binders lose some   of its volatile lower molecular weight constituents   to form carbonyl (- C=O) groups that increase the   polarity of their host compounds. As aging progresses and carbonyl associations are formed, less soluble   asphaltene materials, which behave like solid particles,   are created ( Liu <i>et al</i>., 1998; Jung, 2006). This   composition change increases the asphalt-binder's   viscosity and elastic properties, i.e., the asphaltbinder   loses its viscoelastic and plasticity properties.  </p>     ]]></body>
<body><![CDATA[<p>Thus, the aged asphalt-binder sustains shear   stress with deformation (high elastic stiffness) and   simultaneously, the material cannot relieve the stress   by flow (high viscosity), resulting in asphalt-binder   age-hardening and embrittlement with time. Detailed   chemistry of the asphalt-binder composition and   chemical kinetics (aging) can be found elsewhere   (Domke, Davison and Glover, 2000; Glover <i>et al</i>.,   2005; Jung, 2006).</p>     <p><font size="3"><b>2.2 Asphalt-binder aging and HMA   mixes</b></font></p>     <p>In HMA mixes, asphalt-binder is predominantly   used as a cementitious-bonding material   between the aggregate particles. It is also used as   an HMA waterproofing material. In fact, the HMA   pavement construction industry uses approximately   85 % of the asphalt-binders produced worldwide;   with the asphalt-binder constituting about 4 to 8 % by   weight of the total HMA mix and contributing about   30 % to the total cost of HMA pavement structures   (Jung, 2006).</p>     <p>The oxidative and polarity state of the asphaltbinder   at any given time has a significant bearing on   the chemical, mechanical, and physical properties of   HMA mix, and ultimately, the HMA mix performance   and durability. Due to aging (i.e., increase in polarity)   and changing environmental conditions, the asphaltbinder   age-hardens (stiffens), becomes more brittle,   and loses its viscoelastic properties (Jung, 2006). These changes impact the HMA mix fracture properties   and cracking-resistance potential and increase   the susceptibility of HMA mix to moisture damage   (stripping) and potholing. This change in moisture   susceptibility is because aged asphalt-binders have   a larger number of polar constituents that are more   prone to attracting water molecules; and thus, ease   breakage of the bonding with aggregates (Glover <i>et al</i>., 2005; Jung, 2006).</p>     <p><font size="3"><b>3. THE DIRECT-TENSION  (DT) TEST PROTOCOL</b></font></p>     <p>In this study, the uniaxial DT test was used to   measure the fracture parameters (tensile strength,   strain, tensile modulus, and fracture energy) as a   means to characterize and evaluate the ductility and cracking resistance potential of HMA mixes in   response to aging. The DT test parameters consisted   of a continuous axial tensile load applied at a displacement   rate of 1.27 mm/min (Walubita, 2006).   Under this testing condition, the test took at most 5   minutes. <a href="#fig1">Figure 1</a> shows the laboratory test set-up   and loading configuration for the DT test conducted   in this study (Walubita, Simate and Oh, 2010).</p>     <p>The DT test was conducted at 20 &deg;C with a minimum   temperature pre-conditioning time of 2 hours.   This temperature was monitored via a thermocouple   probe attached inside a dummy HMA mix specimen   also placed in the same environmental-temperature   chamber as the test specimens.</p>     <p><font size="3"><b>4. DT TEST DATA AND ANALYSIS MODELS</b></font></p>     <p>Based on the DT test output data, the HMA   mix tensile strength (<i>&sigma;<sub>t</sub></i>) in MPa, tensile strain at the   peak failure load (<i>&epsilon;<sub>f</sub></i>) in mm/mm, tensile modulus   (<i>E<sub>t</sub></i>) in MPa, fracture energy (<i>G<sub>f(DT)</sub></i>) in J/m<sup>2</sup>, and fracture   energy indices (<i>FE<sub>&sigma;</sub></i> Index and <i>FE<sub>E</sub></i> Index), were   calculated using <a href="#for1">equation 1</a> through <a href="#for6">6</a>, respectively.  </p>       <p align="center"><img src="img/revistas/eia/n17/n17a16for1.gif"><a name="for1"></a></p>     ]]></body>
<body><![CDATA[<p>where <i>P<sub>max</sub></i> is the maximum tensile load at failure   (kN) (or peak failure load, which defines the "failure   condition" or break point of the specimen under DT   testing); <i>r</i> is the specimen radius (mm), i.e., 50 mm   in this case; <i>&Delta;L</i> is the maximum elongation at <i>P<sub>max</sub></i>   (mm); and <i>L<sub>0</sub></i> is the initial centre-to-centre distance   between the linear variable displacement transducers   (LVDTs) (mm), which was 100 mm in this study   (<a href="#fig2">figure 2</a>) (Walubita, 2006; Walubita, Simate and   Oh, 2010).</p>       <p align="center"><img src="img/revistas/eia/n17/n17a16fig2.gif"><a name="fig2"></a></p>     <p>Based on <a href="#for1">equation 4</a>, the total fracture energy   (energy required to fracture the HMA mix specimen)   is represented by the area under the load versus   displacement curve (i.e., area between the integral   limits <i>x<sub>1</sub></i> and <i>x<sub>2</sub></i> in the <a href="#fig2">figure 2</a>). In this study, the fracture   energy was computed only up to the point of peak   failure load that corresponds to part "A" in <a href="#fig2">figure 2</a>,   since the DT tests were terminated at the instance of   50 % drop in the peak failure load. Corresponding   computations of fracture energy were conducted using   the MATLAB (MathWorks, 2011) routine software.</p>     <p><font size="3"><b>5. EXPERIMENTAL DESIGN PLAN</b></font></p>     <p>Two dense-graded HMA mixes that are commonly   used in Texas (USA) were evaluated in this   study. Corresponding mix design characteristics are   listed in <a href="#tab1">table 1</a> and the aggregate gradations are   comparatively shown in <a href="#fig3">figure 3</a> (Walubita, 2006).</p>       <p align="center"><img src="img/revistas/eia/n17/n17a16tab1.gif"><a name="tab1"></a></p>       <p align="center"><img src="img/revistas/eia/n17/n17a16fig3.gif"><a name="fig3"></a></p>     <p>The two HMA mixes listed in <a href="#tab2">table 2</a> were   designed in the laboratory based on the Texas   gyratory compactor and Superpave mix-design   methods (TxDOT, 2011). As shown in the <a href="#fig2">figure 2</a>,   the DT test specimens are cylindrically shaped with   dimensions of 50 mm radius by 150 mm in height;   giratory molded to a target total air void content of   7&plusmn;0.5 % (Walubita, 2006; TxDOT, 2011) to simulate   the field air void content after construction and   trafficking when fatigue-cracking-resistance is considered   critical.</p>       <p align="center"><img src="img/revistas/eia/n17/n17a16tab2.gif"><a name="tab2"></a></p>     <p>As recommended in previous research (Walubita <i>et al</i>., 2012), these DT specimens are typically   cored from 75 mm in radius samples of higher height   (i.e., height &gt; 150 mm) to improve the homogeneity   of the air void distribution (i.e., homogeneity of the   mix internal structure). A minimum of three replicate   specimens were tested for each HMA mix type per   laboratory aging condition and the results subsequently   presented correspond to the mean computed   based on the three replicates. In total, a minimum   of 18 HMA mix samples were molded and tested.</p>     ]]></body>
<body><![CDATA[<p>In order to investigate the suitability of the   DT test to assess the effects of asphalt-binder aging   on the HMA mix fracture parameters and crackingresistance   potential, HMA mix specimens were   exposed to accelerated laboratory aging prior to DT   testing. Three aging exposure conditions (i.e., 0, 3,   and 6 months at 60 &deg;C), that simulate different Texas   field HMA pavement aging at the critical pavement   service temperature based on a study by Glover <i>et al</i>. (2005), were used.</p>     <p>The accelerated aging process of the HMA mix   specimens involved keeping them in a temperaturecontrolled   room at 60 &deg;C and allowing heated air   to circulate freely around the specimens. Previous   research showed that aging of the asphalt-binder   within the HMA specimens occurred under these   laboratory aging conditions (Glover <i>et al</i>., 2005).   Note that all the loose HMA mixes were subjected to   the standard 4 hour short-term oven aging (STOA)   process at 135 &deg;C consistent with the AASHTO PP2   (1994) procedure for Superpave mix performance   testing prior to HMA mix specimen compaction and   the stated 60 &deg;C accelerated aging process. <a href="#tab2">Table 2</a>  summarizes the laboratory aging processes along   with the corresponding references.</p>     <p><font size="3"><b>6. RESULTS AND ANALYSES</b></font></p>     <p>This section presents the results and corresponding   analyses of the laboratory aging effects   on the HMA mix response evaluated in terms of the   fracture parameters computed based on the DT test   data. The first subsection focuses on the analysis of   the tensile strength, tensile strain, and tensile modulus,   followed by analysis of the fracture energy and   the associated indices. It should be noted that these   results pertain only to the HMA mixes, DT test conditions,   and laboratory aging conditions defined in this   study. Therefore, the overall findings and conclusions   may not be exhaustive.</p>     <p><font size="3"><b>6.1 Analysis of tensile strength,   tensile strain, and tensile   modulus</b></font></p>     <p><a href="#fig4">Figure 4</a> shows the stress-strain response of the   HMA mixes as a function of the three different aging   exposure conditions, namely 0, 3, and 6 months.   Overall, the stress-strain response of the mixes is   consistent with theoretical expectations and supports   the preceding discussions about asphalt-binder aging   and embrittlement.</p>       <p align="center"><img src="img/revistas/eia/n17/n17a16fig4.gif"><a name="fig4"></a></p>     <p>As aforementioned, the changes in the asphaltbinder   chemistry and kinetic composition due to aging   leads to age-hardening and embrittlement that,   as evident in <a href="#fig4">figure 4</a>, has a significant impact on the   HMA mix stress-strain response and, consequently,   the cracking resistance potential of the HMA mixes.   As stated in the introduction, however, quantifying   and/or evaluating the actual changes in the chemistry   and kinetic composition of the asphalt-binder or   degree of oxidation due to aging were beyond the   scope of this study.</p>     <p><a href="#fig5">Figure 5</a> shows the values of the tensile   strength and tensile strain at peak failure load for   the HMA mixes evaluated (<a href="#tab2">table 2</a>). In this study, the   tensile strength was adapted as an indicator of the   ultimate tensile load capacity for the HMA mix and   the tensile strain at peak failure load was adapted as   an indicator of the HMA mix ductility potential, which   basically defines the HMA mix's potential to elongate   under tensile stress prior to breakage. Therefore, desirable   ductile mixes are associated with high values   of tensile strain at peak failure load and vice versa   for brittle mixes.</p>       <p align="center"><img src="img/revistas/eia/n17/n17a16fig5.gif"><a name="fig5"></a></p>     ]]></body>
<body><![CDATA[<p>In previous research, Walubita <i>et al</i>. (2010)   suggested discrimination of cracking resistant and not   cracking resistant HMA mixes based on a threshold   value of 3000 &micro;e for the tensile strain at failure; i. e.,   &epsilon;<i><sub>f</sub></i> &ge; 3000 &micro;&epsilon; is related to cracking resistant mixes   under the discussed DT test protocol. This laboratory   criterion exhibited potential to discriminate the   cracking resistance of HMA mixes that also closely   correlated with the observed field performance of   the majority of the HMA mixes evaluated by Walubita   (2006). Based on this previous research and   <a href="#fig4">Figure 4</a>. Comparison of HMA mix stress-strain responses   taking due cognizance of the fact that the tensile   strain at failure does not really constitute a fundamental   quantification of HMA mix ductility, this   fracture parameter was nonetheless adapted as an   indicator of the HMA mix ductility potential for easy   comparison of the mixes.</p>     <p>Based on the previously discussed concepts   in this paper, the data shown in <a href="#fig5">figure 5</a> provide evidence   of changes in the HMA mix fracture response   due to aging. For the mixes evaluated, the tensile   strength increased with aging time. In addition, both   mixes also did not meet the ductility criterion of   &epsilon;<i><sub>f</sub></i> &ge; 3000 &micro;&epsilon; at zero-month aging exposure condition.   In fact, these mixes are classified as moderately   crack resistant based on previous research   studies and actual field performance on Texas   (USA) roads (TxDOT, 2004; Walubita and Scullion,   2008; Walubita, Simate and Oh, 2010). Despite   this observation, the aging effect -reduction of the   mix ductility as evaluated in terms of lower tensile   strain values- were consistently manifested in the   mix response and were sufficiently captured by the   DT test (<a href="#fig5">figure 5b</a>).</p>     <p>Compared to the tensile strength, the reduction   of the tensile strain values is quite substantial with   a likelihood of expecting similar changes in the HMA   mix ductility and cracking resistance potential. For   instance, while the changes in both parameters were   almost similar (approximately 24 %) at 3 months of   aging exposure, the tensile strain had decreased by   70 % in the 6<sup>th</sup> month, while the incremental change   in the tensile strength was only 48 %. Conclusively,   these results indicate that the tensile strain parameter   is more sensitive to aging than that of the tensile   strength. Between the two, the tensile strain at peak   failure load would, therefore, be the best fracture   parameter to use to evaluate the effects of aging on   HMA mixes under DT testing. This conclusion is also   consistent with previous research findings on un-aged   HMA mixes from the authors.</p>     <p><a href="#fig6">Figure 6</a> shows the computed HMA mix   tensile modulus (i.e., secant modulus) as a function   of the three laboratory aging exposure conditions,   namely 0, 3, and 6 months at 60 &deg;C. As theoretically   expected and consistent with the preceding theory   on age-hardening and embrittlement (Jung, 2006),   these DT test results indicate that the HMA mix stiffness   increases as aging progresses. The final stiffness   computed after 6 months of laboratory aging -simulating   the aging induced by approximately 6 to 12   years of Texas HMA mix environmental exposure   (Glover <i>et al</i>., 2005)- is more than five times higher in   magnitude than the stiffness computed for the same   mix evaluated just after laboratory compaction (i.e.,   0 months) -simulating the HMA mix aging condition   just after in situ field compaction (Glover <i>et al</i>.,   2005)-. That is the HMA mix stiffness had increased   by over 100 % by the 6<sup>th</sup> month of laboratory aging.  </p>       <p align="center"><img src="img/revistas/eia/n17/n17a16fig6.gif"><a name="fig6"></a></p>     <p>Compared to the tensile strain (<a href="#fig5">figure 5</a>), <a href="#fig6">figure   6</a> shows that the tensile modulus is comparatively   more sensitive to aging. By the 6<sup>th</sup> month of laboratory   aging, for instance, the change in the tensile   modulus for both mixes was about 5 times to the corresponding   value computed at 0 months aging, while   it was only 3 times for the tensile strain. Between the   two fracture parameters, however, the tensile strain   would be preferred as it is directly related to HMA   ductility potential and also, as reported in previous   publications (Walubita, 2006; Walubita <i>et al</i>., 2010),   it exhibited better correlation with field cracking   performance.</p>     <p>In terms of the particular HMA mix response,   the Superpave mix showed to be more ductile, less   stiff, and exhibited higher ultimate tensile load capacity   than the Type C mix. The higher AC content,   higher asphalt-binder PG grade, and modification   with an SBS polymer along with the use of hydrated   lime (<a href="#tab1">table 1</a>) can partially explain the better ductility response of the Superpave mix. Since the aggregate   gradation did not differ significantly, another factor   leading to the superiority of the Superpave mix   could be the better quality aggregate type (gravel)   used, which is non-absorptive. Most Central Texas   limestone aggregates are known to be highly absorptive   with a high potential to reduce the net effective   asphalt-binder content, which has a negative effect   on the HMA mix fracture properties and cracking   resistance potential (Walubita <i>et al</i>., 2010). All these   factors may have impacted these results, but were   outside the scope of this study.</p>     <p>In summary, analysis of the fracture parameters   computed based on the DT test data sufficiently reflected   the effects of aging on the HMA mix response   and is consistent with theoretical expectations. Overall,   the tensile strain would be the preferred fracture   parameter to characterize the HMA mix cracking   resistance potential as a function of aging. For the   fracture parameters shown in figure 4 through 6 and   looking at their changes in magnitude as a function   of the laboratory aging conditioning process applied,   the Type C mix appears to be more sensitivity to   aging than the particular Superpave mix evaluated   and would theoretically expected to be more susceptible   to age-related fracture damage and cracking.   Between the two particular mixes evaluated, and assuming   similar field conditions, the Superpave would   thus be preferred over the Type C mix.</p>     <p><font size="3"><b>6.2 Analysis of fracture energy and   fracture energy indices</b></font></p>     <p>The computed fracture energy (FE) and associated   indices are plotted in figures <a href="#fig7">7</a> and <a href="#fig8">8</a>, respectively,   as a function of the tensile strain at peak failure   load and the laboratory aging exposure conditions.   Note that in addition to the FE and the preceding   fracture parameters discussed in Section 6.1, the FE   Index was also explored as a novel concept to gauge   if it provided superior and effective differentiating capabilities   in terms of capturing the HMA mix fracture   response to laboratory aging under DT testing. For   the purpose of this study, the FE Index was devised   and defined as a parametric ratio that quantifies the   amount of fracture energy required to induce damage   relative to the HMA tensile strength and/or stiffness. Mathematically and as indicated in equations   <a href="#for1">5</a> and <a href="#for1">6</a>, the FE Index is computed as a ratio of the   FE to the HMA mix tensile strength and/or stiffness.</p>       ]]></body>
<body><![CDATA[<p align="center"><img src="img/revistas/eia/n17/n17a16fig7.gif"><a name="fig7"></a></p>       <p align="center"><img src="img/revistas/eia/n17/n17a16fig8.gif"><a name="fig8"></a></p>     <p>With the exception of the 3-month data for the   Type C mix, the fracture energy generally exhibits a   decreasing trend with aging as theoretically expected,   implying that as the asphalt-binder losses its cohesive/adhesive and bonding properties due to aging, less   energy is required to induce fracture damage and/or cracking. Theoretically, higher fracture energy   values denote better resistance to fracture damage   and cracking for the HMA mix. Therefore, aging is an   undesired phenomenon in the HMA mixes.</p>     <p>Like <a href="#fig4">figure 4</a> through <a href="#fig6">6</a>, both figures <a href="#fig7">7</a> and <a href="#fig8">8</a>  seem to suggest that the Type C mix, as compared to   the Superpave mix, is more susceptible to fracture   damage and cracking based on the smaller magnitudes   of the FE parameters at all levels of aging. That   is, if all other factors are equal, less energy would   be required to cause fracture damage in the Type C   mix compared to the Superpave mix; it is an aspect   which can be tied to the mix-design characteristics   listed in <a href="#tab1">table 1</a>. In the case of figure <a href="#fig7">7</a>, however, the opposite would be concluded if the interpretation of   the data is purely based on the slopes of graphs. Thus,   the need to focus on the FE Indices that show a more   consistent and distinctive response trend, particularly   the FE<sub>E</sub> Index. Furthermore, although the Type C   mix exhibits an unexplained characteristic response   at 3 months aging, the general trend of the fracture   energy is nonetheless clearly evident; it is decreasing   as a function of laboratory aging time, e.g., Type C-0   months versus Type C-6 months.</p>     <p>Looking at <a href="#fig8">figure 8</a> and considering the fitted   trend lines, it is clear that the FE<sub>E</sub> Index provides   a more distinctive and consistent differentiation of   the HMA mix response as a function of both aging   condition and tensile strain at peak failure load.   Theoretically, this may be attributed to the fact the   FE<sub>E</sub> Index represents a combination of all the HMA   mix fracture parameters (namely <i>FE</i>, s<sub>t</sub>, and e<sub>t</sub>) and   thereby, capturing the complete fracture response of   the HMA mix under DT testing. Therefore, the FE<sub>E</sub>   Index would be preliminarily recommended at this   stage as the suitable fracture parameter to assess the   cracking resistance potential of HMA mixes as a function   of laboratory aging under DT testing. However,   additional research is still required to validate these   results and suggest a final recommendation for future   HMA mix characterization.</p>     <p><a href="#tab3">Table 3</a> is a comparative listing of all the fracture   parameters computed as a function of aging and   provides additional evidence that the Superpave mix has superior fracture response than the Type C mix.   Other than the tensile modulus, all the fracture parameters   for the Superpave mix are desirably higher   in magnitude than the Type C mix at all laboratory   aging conditions.</p>       <p align="center"><img src="img/revistas/eia/n17/n17a16tab3.gif"><a name="tab3"></a></p>     <p>The higher tensile modulus values of the   Type C mix suggests that this mix is relatively stiffer   and more brittle (less ductile) than the Superpave   mix. As noted in <a href="#tab3">table 3</a>, this poor ductility potential   means that the mix sustains lower tensile strains prior   to failure and that relatively lower fracture energy   is expanded to induce this damage. As theoretically   expected, the cracking resistance potential, as   measured by the changes in the fracture parameters   listed in <a href="#tab3">table 3</a>, seems to deteriorate with aging time   for both mixes; with this particular Type C mix (i.e.,   asphalt-aggregate combination) exhibiting more   sensitivity to aging.</p>     <p><font size="3"><b>6.3 Statistical analysis</b></font></p>     <p>In terms of statistical variability of the DT data,   the COV for st ranged from 2 % to 7 %, while the COV   range was from 4 % to 18 % for the <i>&epsilon;<sub>f</sub></i> and <i>E<sub>t</sub></i> parameters.   In general, higher COV values were measured   for the Superpave mix samples at all laboratory aging   conditions, presumably due to poor workability   problems in the laboratory attributed to the stiffer   asphalt-binder due to the SBS modifier (Walubita,   2006). Parameter wise, statistical variability was least   in the computation of <i>&sigma;<sub>t</sub></i> and more scattered for the <i>&epsilon;<sub>f</sub></i> parameter. Assuming a COV threshold of 30 %   (Walubita <i>et al</i>., 2010), these statistics are, therefore,   considered reasonably acceptable to statistically   substantiate the above results and findings.</p>     ]]></body>
<body><![CDATA[<p>Likewise, the COV values for both the FE and   FE Indices exhibited a similar trend and were all less   than 30 % in magnitude. However, they were slightly   higher than the preceding fracture parameters, ranging   from 12 % to 29 %. Nonetheless, the COV values   were still considered reasonable (i.e., less than 30 %)   and thus, further substantiating the statistical validity   of the results and findings presented.  </p>     <p><font size="3"><b>7. CONCLUSIONS AND   RECOMMENDATIONS</b></font></p>     <p>This paper documented a laboratory study   that was conducted to evaluate the suitability of   the direct-tension (DT) test to assess the effects   of asphalt-binder aging on the HMA mix fracture   properties and cracking-resistance potential. Two   dense-graded HMA mixes with different mix-design   characteristics were subjected to three laboratory   aging exposure conditions (0, 3, and 6 months at   60 &deg;C) and then, tested in the DT test to measure   the following fracture parameters: tensile strength,   tensile strain at peak failure load, tensile modulus,   fracture energy, and fracture indices. Analysis of these   fracture parameters as a function of aging yielded the   following conclusions:</p>   <ul type="disc">     <li>Through measurement and computation of the   fracture parameters evaluated, this study suggests   that the DT test (i.e., at 1.27 mm/min load   rate and 20 &deg;C) can successfully be used to characterize   and capture the HMA mix sensitivity to   asphalt-binder aging in the laboratory.</li>     <li>Of the HMA fracture parameters evaluated   based on the DT test, the tensile strain at peak   failure load and the FE<sub>E</sub> Index exhibited the best   potential to capture the effects of aging on the   HMA mix fracture response. Therefore, these   parameters (in particular the FE<sub>E</sub> Index) should   be explored further as a means to characterize   the HMA mix fracture response and sensitivity   to asphalt-binder aging under DT testing.</li>     <li>As a function of aging, the HMA mixes exhibited   the following responses under DT testing: (<a href="#for1">1</a>)   the tensile strength and tensile modulus increased,   (<a href="#for1">2</a>) the tensile strain at peak failure load decreased,   and (<a href="#for1">3</a>) despite one outlier, the fracture   energy required to induce damage generally   exhibited a decreasing trend. This means that   the HMA mixes become more susceptible to   fracture   damage with aging time, which among   other factors can theoretically be attributed   to progressive loss of adhesive/cohesive and   bonding properties as well as changes in the   rheological properties of the asphalt-binder.</li>     <li>Due to the differences in the mix-design variables   of the two particular HMA mixes tested,   the HMA mix response to asphalt-binder aging   was different, with the Superpave mix exhibiting   superior fracture properties and cracking resistance   potential at all aging conditions. Thus,   adequate mix-design (i.e., including proper selection   of the asphalt-aggregate combination) is   one aspect to optimize the HMA mix resistance   to age-related fracture damage and cracking.</li>       </ul>     <p>Overall, this study has demonstrated that aging   is detrimental to the HMA mix fracture properties and   obviously, cracking performance; and that different   HMA mixes respond differently to asphalt-binder aging.   In addition to premature fracture damage and   cracking, potholing and loss of durability are other   distresses likely to be exacerbated by asphalt-binder   aging. Therefore, consideration should be undertaken   to sufficiently incorporate aging in HMA mix   designs and performance prediction models. Development   of new generation mix-design methods and   aging shift factors to account for asphalt-binder aging   are some of the options to consider. Lastly, additional   research is recommended to validate the findings of   this study along with more HMA mixes and correlations   with field performance data.</p>     <p><font size="3"><b>8. ACKNOWLEDGEMENTS</b></font></p>     ]]></body>
<body><![CDATA[<p>This study was conducted as part of TxDOT   and the Federal Highway Administration (FHWA)   sponsored research projects to evaluate different   laboratory HMA mix crack test methods including   effects of aging. The authors grateful acknowledge   and thank TxDOT and FHWA for the financial support.   The authors also thank all those who rendered   help towards the completion of this study as well as   the paper, particularly Gautam Das, Lee Gustavus,   Tony Barbosa, Geoffrey S. Simate (Wits University,   South Africa), Charles Mushota (Estal Pride (Z) Ltd.,   Zambia), and Tom Scullion (TTI) for their invaluable   contributions to this study as the paper itself. The   third author, as Associate Professor of the University   of Magdalena (Colombia), expresses special thanks to   this institution for the support received to complete   this work. Lastly, the primary author also acknowledges   the assistance received from the Wuhan   Institute of Technology (China), where he serves as   a Visiting Professor.</p>     <p><font size="3"><b>9. DISCLAIMER</b></font></p>     <p>The contents of this paper reflect the views of   the authors who are solely responsible for the facts   and accuracy of the data presented herein and do  not necessarily reflect the official views or policies of   any agency or institute. This paper does not constitute   a standard, specification, nor is it intended for   design, construction, bidding, contracting, tendering,   or permit purposes. Trade names were used   solely for information purposes and not for product   endorsement.</p>     <p><font size="3"><b>REFERENCES</b></font></p>     <!-- ref --><p>AASHTO. <i>Standard specifications for transportation materials   and methods of sampling and testing. Designation: PP2,   Standard practice for short and long term aging of hot   mix asphalt</i>. Washington D.C., 1994.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000107&pid=S1794-1237201200010001600001&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Airey, G. D. (2003). "State of the art report on ageing   test methods for bituminous pavement materials".   <i>International Journal of Pavement Engineering</i>, vol. 4,   No. 3, pp. 165-176.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000108&pid=S1794-1237201200010001600002&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Arenas, H. L. <i>Tecnolog&iacute;a del cemento asf&aacute;ltico</i>. Popay&aacute;n:   Faid, 2005.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000109&pid=S1794-1237201200010001600003&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Asphalt Rehab: (consulted on June 11, 2012) Available in:   &lt;<a href="http://www.asphaltrehab.com/infrared.html" target="_blank">http://www.asphaltrehab.com/infrared.html</a>&gt;.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000110&pid=S1794-1237201200010001600004&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Domke, C. H.; Davison, R. R. and Glover, C. J. (2000). "Effect   of oxygen pressure on asphalt oxidation kinetics".   <i>Industrial and Engineering Chemistry Research</i>, vol. 39,   No. 3, pp. 592-598.  &nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000111&pid=S1794-1237201200010001600005&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Glover, C. j.; Davison, R. R.; Domke, C.; Ruan, Y.; Juristyarini,   P.; Knorr, D. and Jung, S. H. <i>Development of a new   method for assessing asphalt binder durability with field   validation</i>. Report No. FHWA/TX-05/1872-2. College   Station, TX: Texas Transportation Institute / Texas A and M   University, 2005.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000112&pid=S1794-1237201200010001600006&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Huang, C.; Abu Al-Rub, R.; Masad, E.; Little, D. and Airey,   G. (2011). "Numerical implementation and validation   of a nonlinear viscoelastic and viscoplastic model   for asphalt mixes". <i>International Journal of Pavement   Engineering</i>, vol. 12, No 4, pp. 433-447.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000113&pid=S1794-1237201200010001600007&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Jung, S. F. <i>The effects of asphalt binder oxidation on hot   mix asphalt concrete mixture rheology and fatigue performance</i>.   Ph.D. Dissertation (Chemical Engineering),   Texas A and M University, College Station, TX, 2006.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000114&pid=S1794-1237201200010001600008&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Kandhal, P. S. and Chakraborty, S. (1996). "Effect of asphalt   film thickness on short- and long-term aging of asphalt   paving mixtures". <i>Transportation Research Record</i>,   No. 1535, pp. 83-90.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000115&pid=S1794-1237201200010001600009&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Kim, R. Y. <i>Modeling of asphalt concrete</i>. New York:   McGraw-Hill, 2009.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000116&pid=S1794-1237201200010001600010&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Lin, M.-S.; Chaffin, J. M.; Liu, M.; Glover, C. J.; Davison, R.   R. and Bullin, J. A. (1996). <i>The effect of asphalt composition   on the formation of asphaltenes and their contribution   to asphalt viscosity</i>. International Symposium on the   Thermodynamics of Heavy Oils and Asphaltenes, Houston,   TX (20 March 1995), vol. 14, No. 1-2, pp. 139-162.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000117&pid=S1794-1237201200010001600011&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Liu, M. M.; Lin, M. S.; Chaffin, J. M.; Davison, R. R.; Glover,   C. J. and Bullin, J. A. (1998). "Oxidation kinetics of asphalt   Corbett fractions and compositional dependence   of asphalt oxidation". <i>Petroleum Science and Technology</i>,   vol. 16, No. 7-8, pp. 827-850.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000118&pid=S1794-1237201200010001600012&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Lu, X. and Isacsson, U. (2002). "Effect of ageing on bitumen   chemistry and rheology". <i>Construction and Building   Materials</i>, vol. 16, No. 1 (February), pp. 15-22.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000119&pid=S1794-1237201200010001600013&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>MathWorks. MATLAB. Natick, Massachusetts, USA, 2011.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000120&pid=S1794-1237201200010001600014&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Pavement Interactive (PI). (consulted on July 8, 2011)   Available at: &lt;<a href="http://pavementinteractive.org/index.php?title=Top-Down_Cracking" target="_blank">http://pavementinteractive.org/index.php?title=Top-Down_Cracking</a>&gt;.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000121&pid=S1794-1237201200010001600015&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Pfeiffer, J. P. and Saal, R. N. J. (1940). "Asphaltic bitumen   as colloid system". <i>The Journal of Physical Chemistry</i>,   vol. 44, No. 2, pp. 139-149.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000122&pid=S1794-1237201200010001600016&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Punith, V. S.; Xiao, F.; Putman, B. and Amirkhanian, S. N.   (2012). "Effects of long-term aging on moisture sensitivity   of foamed WMA mixtures containing moist aggregates".   <i>Materials and Structures</i>, vol. 45, pp. 251-264.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000123&pid=S1794-1237201200010001600017&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>TxDOT Standard specifications for construction and   maintenance of highways, streets, and bridges. Austin,   TX, 2004.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000124&pid=S1794-1237201200010001600018&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>TxDOT. TxDot online manuals (consulted on July 2, 2011)   Available in: &lt;<a href="http://www.dot.state.tx.us/services/general_services/manuals.htm" target="_blank">http://www.dot.state.tx.us/services/general_services/manuals.htm</a>&gt;.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000125&pid=S1794-1237201200010001600019&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Vargas, X. and Reyes, F. (2010). "Asphalt's aging phenomenon".   <i>Ingenier&iacute;a e Investigaci&oacute;n</i>, vol. 30, No. 3,   pp. 27-44.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000126&pid=S1794-1237201200010001600020&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Walubita, L. F. Comparison of fatigue analysis approaches   for predicting fatigue lives of hot-mix asphalt concrete   (HMAC) mixtures. PhD Dissertation, Texas A and M University,   College Station, TX, 2006.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000127&pid=S1794-1237201200010001600021&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Walubita, L. F.; Jamison, B.; Alvarez, A. E.; Hu, X. and   Mushota, C. (2012). "Air void characterisation of HMA   gyratory laboratory-moulded samples and field cores   using X-ray computed tomography (X-ray ct)". <i>Journal   of the South African Institution of Civil Engineering</i>,   vol. 54, No. 1 (April), pp. 22-31.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000128&pid=S1794-1237201200010001600022&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Walubita, L. F. and Scullion, T. <i>Thin HMA overlays in   Texas: Mix-design and laboratory material property   characterization. Research Report No 0-5598-1</i>. Texas   Transportation Institute-Texas A and M University, College   Station, TX, 2008.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000129&pid=S1794-1237201200010001600023&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Walubita, L. F.; Simate, G. S. and Oh, J. (2010). "Characterising   the ductility and fatigue crack resistance potential   of asphalt mixes based on the laboratory direct tensile   strength test". <i>Journal of the South African Institution of   Civil Engineering</i>, vol. 52, No. 2, pp. 31-40.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000130&pid=S1794-1237201200010001600024&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --><!-- ref --><p>Walubita, L. F.; Umashankar, V.; Hu, X.; Jamison, B.; Zhou,   F.; Scullion, T.; Epps Martin, A. and Dessouky, S. <i>New   generation mix-designs: Laboratory testing and construction   of the apt test sections. Report 0-6132-1</i>. Texas   Transportation Institute-Texas A and M University, College   Station, TX, 2010.&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=000131&pid=S1794-1237201200010001600025&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --> ]]></body><back>
<ref-list>
<ref id="B1">
<nlm-citation citation-type="">
<collab>AASHTO</collab>
<source><![CDATA[Standard specifications for transportation materials and methods of sampling and testing. Designation: PP2, Standard practice for short and long term aging of hot mix asphalt]]></source>
<year>1994</year>
<publisher-loc><![CDATA[Washington^eD.C. D.C.]]></publisher-loc>
</nlm-citation>
</ref>
<ref id="B2">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Airey]]></surname>
<given-names><![CDATA[G. D]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[State of the art report on ageing test methods for bituminous pavement materials]]></article-title>
<source><![CDATA[International Journal of Pavement Engineering]]></source>
<year>2003</year>
<volume>4</volume>
<numero>3</numero>
<issue>3</issue>
<page-range>165-176</page-range></nlm-citation>
</ref>
<ref id="B3">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Arenas]]></surname>
<given-names><![CDATA[H. L]]></given-names>
</name>
</person-group>
<source><![CDATA[Tecnología del cemento asfáltico]]></source>
<year>2005</year>
<publisher-loc><![CDATA[Popayán ]]></publisher-loc>
<publisher-name><![CDATA[Faid]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B4">
<nlm-citation citation-type="">
<collab>Asphalt Rehab</collab>
<source><![CDATA[]]></source>
<year></year>
</nlm-citation>
</ref>
<ref id="B5">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Domke]]></surname>
<given-names><![CDATA[C. H]]></given-names>
</name>
<name>
<surname><![CDATA[Davison]]></surname>
<given-names><![CDATA[R. R]]></given-names>
</name>
<name>
<surname><![CDATA[Glover]]></surname>
<given-names><![CDATA[C. J]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Effect of oxygen pressure on asphalt oxidation kinetics]]></article-title>
<source><![CDATA[Industrial and Engineering Chemistry Research]]></source>
<year>2000</year>
<volume>39</volume>
<numero>3</numero>
<issue>3</issue>
<page-range>592-598</page-range></nlm-citation>
</ref>
<ref id="B6">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Glover]]></surname>
<given-names><![CDATA[C. j]]></given-names>
</name>
<name>
<surname><![CDATA[Davison]]></surname>
<given-names><![CDATA[R. R]]></given-names>
</name>
<name>
<surname><![CDATA[Domke]]></surname>
<given-names><![CDATA[C]]></given-names>
</name>
<name>
<surname><![CDATA[Ruan]]></surname>
<given-names><![CDATA[Y]]></given-names>
</name>
<name>
<surname><![CDATA[Juristyarini]]></surname>
<given-names><![CDATA[P]]></given-names>
</name>
<name>
<surname><![CDATA[Knorr]]></surname>
<given-names><![CDATA[D]]></given-names>
</name>
<name>
<surname><![CDATA[Jung]]></surname>
<given-names><![CDATA[S. H]]></given-names>
</name>
</person-group>
<source><![CDATA[Development of a new method for assessing asphalt binder durability with field validation]]></source>
<year>2005</year>
<publisher-loc><![CDATA[College Station^eTX TX]]></publisher-loc>
<publisher-name><![CDATA[Texas Transportation InstituteTexas A and M University]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B7">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Huang]]></surname>
<given-names><![CDATA[C]]></given-names>
</name>
<name>
<surname><![CDATA[Abu Al-Rub]]></surname>
<given-names><![CDATA[R]]></given-names>
</name>
<name>
<surname><![CDATA[Masad]]></surname>
<given-names><![CDATA[E]]></given-names>
</name>
<name>
<surname><![CDATA[Little]]></surname>
<given-names><![CDATA[D]]></given-names>
</name>
<name>
<surname><![CDATA[Airey]]></surname>
<given-names><![CDATA[G]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Numerical implementation and validation of a nonlinear viscoelastic and viscoplastic model for asphalt mixes]]></article-title>
<source><![CDATA[International Journal of Pavement Engineering]]></source>
<year>2011</year>
<volume>12</volume>
<numero>4</numero>
<issue>4</issue>
<page-range>433-447</page-range></nlm-citation>
</ref>
<ref id="B8">
<nlm-citation citation-type="">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Jung]]></surname>
<given-names><![CDATA[S. F]]></given-names>
</name>
</person-group>
<source><![CDATA[The effects of asphalt binder oxidation on hot mix asphalt concrete mixture rheology and fatigue performance]]></source>
<year></year>
</nlm-citation>
</ref>
<ref id="B9">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Kandhal]]></surname>
<given-names><![CDATA[P. S]]></given-names>
</name>
<name>
<surname><![CDATA[Chakraborty]]></surname>
<given-names><![CDATA[S]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Effect of asphalt film thickness on short- and long-term aging of asphalt paving mixtures]]></article-title>
<source><![CDATA[Transportation Research Record]]></source>
<year>1996</year>
<numero>1535</numero>
<issue>1535</issue>
<page-range>83-90</page-range></nlm-citation>
</ref>
<ref id="B10">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Kim]]></surname>
<given-names><![CDATA[R. Y]]></given-names>
</name>
</person-group>
<source><![CDATA[Modeling of asphalt concrete]]></source>
<year>2009</year>
<publisher-loc><![CDATA[New York ]]></publisher-loc>
<publisher-name><![CDATA[McGraw-Hill]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B11">
<nlm-citation citation-type="confpro">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Lin]]></surname>
<given-names><![CDATA[M.-S]]></given-names>
</name>
<name>
<surname><![CDATA[Chaffin]]></surname>
<given-names><![CDATA[J. M]]></given-names>
</name>
<name>
<surname><![CDATA[Liu]]></surname>
<given-names><![CDATA[M]]></given-names>
</name>
<name>
<surname><![CDATA[Glover]]></surname>
<given-names><![CDATA[C. J]]></given-names>
</name>
<name>
<surname><![CDATA[Davison]]></surname>
<given-names><![CDATA[R. R]]></given-names>
</name>
<name>
<surname><![CDATA[Bullin]]></surname>
<given-names><![CDATA[J. A]]></given-names>
</name>
</person-group>
<source><![CDATA[The effect of asphalt composition on the formation of asphaltenes and their contribution to asphalt viscosity]]></source>
<year>1996</year>
<volume>14</volume>
<conf-name><![CDATA[ International Symposium on the Thermodynamics of Heavy Oils and Asphaltenes]]></conf-name>
<conf-date>20 March 1995</conf-date>
<conf-loc>Houston TX</conf-loc>
<page-range>139-162</page-range></nlm-citation>
</ref>
<ref id="B12">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Liu]]></surname>
<given-names><![CDATA[M. M]]></given-names>
</name>
<name>
<surname><![CDATA[Lin]]></surname>
<given-names><![CDATA[M. S]]></given-names>
</name>
<name>
<surname><![CDATA[Chaffin]]></surname>
<given-names><![CDATA[J. M]]></given-names>
</name>
<name>
<surname><![CDATA[Davison]]></surname>
<given-names><![CDATA[R. R]]></given-names>
</name>
<name>
<surname><![CDATA[Glover]]></surname>
<given-names><![CDATA[C. J]]></given-names>
</name>
<name>
<surname><![CDATA[Bullin]]></surname>
<given-names><![CDATA[J. A]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Oxidation kinetics of asphalt Corbett fractions and compositional dependence of asphalt oxidation]]></article-title>
<source><![CDATA[Petroleum Science and Technology]]></source>
<year>1998</year>
<volume>16</volume>
<numero>7-8</numero>
<issue>7-8</issue>
<page-range>827-850</page-range></nlm-citation>
</ref>
<ref id="B13">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Lu]]></surname>
<given-names><![CDATA[X]]></given-names>
</name>
<name>
<surname><![CDATA[Isacsson]]></surname>
<given-names><![CDATA[U]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Effect of ageing on bitumen chemistry and rheology]]></article-title>
<source><![CDATA[Construction and Building Materials]]></source>
<year>2002</year>
<month>Fe</month>
<day>br</day>
<volume>16</volume>
<numero>1</numero>
<issue>1</issue>
<page-range>15-22</page-range></nlm-citation>
</ref>
<ref id="B14">
<nlm-citation citation-type="">
<collab>MathWorks</collab>
<source><![CDATA[MATLAB]]></source>
<year>2011</year>
<publisher-loc><![CDATA[Natick^eMassachusetts Massachusetts]]></publisher-loc>
</nlm-citation>
</ref>
<ref id="B15">
<nlm-citation citation-type="">
<collab>Pavement Interactive</collab>
<source><![CDATA[]]></source>
<year></year>
</nlm-citation>
</ref>
<ref id="B16">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Pfeiffer]]></surname>
<given-names><![CDATA[J. P]]></given-names>
</name>
<name>
<surname><![CDATA[Saal]]></surname>
<given-names><![CDATA[R. N. J]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Asphaltic bitumen as colloid system]]></article-title>
<source><![CDATA[The Journal of Physical Chemistry]]></source>
<year>1940</year>
<volume>44</volume>
<numero>2</numero>
<issue>2</issue>
<page-range>139-149</page-range></nlm-citation>
</ref>
<ref id="B17">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Punith]]></surname>
<given-names><![CDATA[V. S]]></given-names>
</name>
<name>
<surname><![CDATA[Xiao]]></surname>
<given-names><![CDATA[F]]></given-names>
</name>
<name>
<surname><![CDATA[Putman]]></surname>
<given-names><![CDATA[B]]></given-names>
</name>
<name>
<surname><![CDATA[Amirkhanian]]></surname>
<given-names><![CDATA[S. N]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Effects of long-term aging on moisture sensitivity of foamed WMA mixtures containing moist aggregates]]></article-title>
<source><![CDATA[Materials and Structures]]></source>
<year>2012</year>
<volume>45</volume>
<page-range>251-264</page-range></nlm-citation>
</ref>
<ref id="B18">
<nlm-citation citation-type="">
<collab>TxDOT</collab>
<source><![CDATA[Standard specifications for construction and maintenance of highways, streets, and bridges]]></source>
<year>2004</year>
<publisher-loc><![CDATA[Austin^eTX TX]]></publisher-loc>
</nlm-citation>
</ref>
<ref id="B19">
<nlm-citation citation-type="">
<collab>TxDOT</collab>
<source><![CDATA[TxDot online manuals]]></source>
<year></year>
</nlm-citation>
</ref>
<ref id="B20">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Vargas]]></surname>
<given-names><![CDATA[X]]></given-names>
</name>
<name>
<surname><![CDATA[Reyes]]></surname>
<given-names><![CDATA[F]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Asphalt's aging phenomenon]]></article-title>
<source><![CDATA[Ingeniería e Investigación]]></source>
<year>2010</year>
<volume>30</volume>
<numero>3</numero>
<issue>3</issue>
<page-range>27-44</page-range></nlm-citation>
</ref>
<ref id="B21">
<nlm-citation citation-type="">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Walubita]]></surname>
<given-names><![CDATA[L. F]]></given-names>
</name>
</person-group>
<source><![CDATA[Comparison of fatigue analysis approaches for predicting fatigue lives of hot-mix asphalt concrete (HMAC) mixtures]]></source>
<year></year>
</nlm-citation>
</ref>
<ref id="B22">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Walubita]]></surname>
<given-names><![CDATA[L. F]]></given-names>
</name>
<name>
<surname><![CDATA[Jamison]]></surname>
<given-names><![CDATA[B]]></given-names>
</name>
<name>
<surname><![CDATA[Alvarez]]></surname>
<given-names><![CDATA[A. E]]></given-names>
</name>
<name>
<surname><![CDATA[Hu]]></surname>
<given-names><![CDATA[X]]></given-names>
</name>
<name>
<surname><![CDATA[Mushota]]></surname>
<given-names><![CDATA[C]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Air void characterisation of HMA gyratory laboratory-moulded samples and field cores using X-ray computed tomography (X-ray ct)]]></article-title>
<source><![CDATA[Journal of the South African Institution of Civil Engineering]]></source>
<year>2012</year>
<month>Ap</month>
<day>ri</day>
<volume>54</volume>
<numero>1</numero>
<issue>1</issue>
<page-range>22-31</page-range></nlm-citation>
</ref>
<ref id="B23">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Walubita]]></surname>
<given-names><![CDATA[L. F]]></given-names>
</name>
<name>
<surname><![CDATA[Scullion]]></surname>
<given-names><![CDATA[T]]></given-names>
</name>
</person-group>
<source><![CDATA[Thin HMA overlays in Texas: Mix-design and laboratory material property characterization]]></source>
<year>2008</year>
<publisher-loc><![CDATA[College Station^eTX TX]]></publisher-loc>
<publisher-name><![CDATA[Texas Transportation InstituteTexas A and M University]]></publisher-name>
</nlm-citation>
</ref>
<ref id="B24">
<nlm-citation citation-type="journal">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Walubita]]></surname>
<given-names><![CDATA[L. F]]></given-names>
</name>
<name>
<surname><![CDATA[Simate]]></surname>
<given-names><![CDATA[G. S]]></given-names>
</name>
<name>
<surname><![CDATA[Oh]]></surname>
<given-names><![CDATA[J]]></given-names>
</name>
</person-group>
<article-title xml:lang="en"><![CDATA[Characterising the ductility and fatigue crack resistance potential of asphalt mixes based on the laboratory direct tensile strength test]]></article-title>
<source><![CDATA[Journal of the South African Institution of Civil Engineering]]></source>
<year>2010</year>
<volume>52</volume>
<numero>2</numero>
<issue>2</issue>
<page-range>31-40</page-range></nlm-citation>
</ref>
<ref id="B25">
<nlm-citation citation-type="book">
<person-group person-group-type="author">
<name>
<surname><![CDATA[Walubita]]></surname>
<given-names><![CDATA[L. F]]></given-names>
</name>
<name>
<surname><![CDATA[Umashankar]]></surname>
<given-names><![CDATA[V]]></given-names>
</name>
<name>
<surname><![CDATA[Hu]]></surname>
<given-names><![CDATA[X]]></given-names>
</name>
<name>
<surname><![CDATA[Jamison]]></surname>
<given-names><![CDATA[B]]></given-names>
</name>
<name>
<surname><![CDATA[Zhou]]></surname>
<given-names><![CDATA[F]]></given-names>
</name>
<name>
<surname><![CDATA[Scullion]]></surname>
<given-names><![CDATA[T]]></given-names>
</name>
<name>
<surname><![CDATA[Epps Martin]]></surname>
<given-names><![CDATA[A]]></given-names>
</name>
<name>
<surname><![CDATA[Dessouky]]></surname>
<given-names><![CDATA[S]]></given-names>
</name>
</person-group>
<source><![CDATA[New generation mix-designs: Laboratory testing and construction of the apt test sections]]></source>
<year>2010</year>
<publisher-loc><![CDATA[College Station^eTX TX]]></publisher-loc>
<publisher-name><![CDATA[Texas Transportation InstituteTexas A and M University]]></publisher-name>
</nlm-citation>
</ref>
</ref-list>
</back>
</article>
